Determination of 90Sr in different matrices via ion-exchange chromatography and LSC

Journal of Radioanalytical and Nuclear Chemistry - A cation-exchange chromatographic method was utilized to isolate strontium. The interference of recovery yield, calcium and magnesium, and the...     

锌电极放电过程及失效机制数值分析

锌-空气电池是一种高能量的电池体系.实验表明, 在大功率工作条件下, 锌电极的材料利用率随电流密度的增加而急剧下降. 为探索其在大功率工作条件下的放电机理, 本文针对这一过程建立了一维数学模型, 通过数值求解模拟多个物理量如离子浓度、传递电流密度、电极孔隙度、固体氧化锌等在电极内部的分布变化情况, 在此基础上分析电极的性能. 数值结果分析表明, 固体氧化锌对电极内质量传输过程的限制是导致电极失效的根本原因. 其析出时间及在电极内部的集中分布位置对电极性能有显著影响; 而仅当其体积分数超过30%-35%的范围后才开始显著限制传质过程. 讨论了电极的优化措施, 模拟表明更高的溶液电导率,更大的电极孔隙度有利于增加大功率工作条件下电极的材料利用率. 但最重要的是保持电极内部氢氧根离子的浓度在一个较高的值,对于封闭式电极可以通过补液实现, 理想情况为设计一个电解液循环式的锌电极.     

基于FPGA的脉冲电源及其控制系统设计

针对等离子体特定领域的应用需求,研制了一种基于上位机监控且具有手动/自动控制功能的脉冲电源。详细介绍了脉冲电源主电路、检测电路、驱动电路、数字脉宽调制(DPWM)产生模块以及脉冲变压器的设计方法。该电源采用现场可编程门阵列(FPGA)作为主控芯片,产生DPWM信号及继电器控制信号,经驱动电路放大后驱动逆变全桥及继电器。设计了过温和短路保护电路,通过DS18B20温度传感器和QBC10PS5霍尔电流传感器对电源模块的工作温度和电流进行实时采样。实际应用测试表明,该电源满足设计指标要求。     

Fabrication of flame-retardant and smoke-suppressant isocyanate-based polyimide foam modified by silica aerogel thermal insulation and flame protection layers

Because of containing urea groups, flame resistance and smoke releasing behaviors of isocyanate-based polyimide foam (IBPIF) produced using free foaming technology require further improvement. In this work, silica aerogel layers were incorporated into cells of IBPIF through an in situ growth process of silica sol (SS). Compared with silica aerogel particles directly mixed into the foaming slurry, the silica aerogel layers that firmly attached to the pores and surfaces of cells not only provided exceptional thermal insulation and flame protection, but also kept original cellular structure. With increase in ratio of SS mass to IBPIF volume, silica aerogel incorporation dosage was gradually increased. Accompanied by flame resistance was obviously improved and smoke releasing behavior was effectively suppressed. Those were indicated by the improved limiting oxygen index (LOI), decreased heat release rate (HRR), peak of HRR, and specific optical density of smoke (Ds) in trials with pilot flames. Compared with pure IBPIF, when the ratio reached to 5/15 g/cm³, it resulted in LOI increasing from 22.0% to 33.0%, peak of HRR, total smoke production (TSP), and maximum value of Ds decreasing from 174 to 72 kW/m², 1.11 to 0.37 m²/m², 45.90 to 17.45, respectively.     

Brewster Angle Effect on Performances of a New Millimeter Wave Omni-Directional Antenna Gloved with a Dielectric Shell

A new millimeter-wave omni-directional antenna consisting of circular rod corrugations gloved with a dielectric shell operating in the TM₀₁ mode is investigated. As an eigenvalue problem, the antenna is analyzed with the rigorous mode matching method. The radiation characteristics of the antenna are calculated for different parameters with a particular attention directed to the Brewster angle effect on the performances of the antenna. A comparison of the radiation characteristics is made between the antennas with and without dielectric shell. It is found that the introduction of the dielectric shell will change the location where the leakage constant reduced to zero. The effectiveness and reliability of the present analysis are verified by the calculated results given in the literature. Therefore, some useful guidelines for the design of the antenna are thereby suggested.     

DYNAMICAL ANALYSIS OF A CYLINDRICAL PIEZOELECTRIC TRANSDUCER

In the present paper, the vibration of a cylindrical piezoelectric transducer induced by applied voltage, which can be used as the stator transducer of a cylindrical micromotor, is studied based on shell theory. The transducer is modelled as a thin elastic cylinder. The properties of the vibration modes of the transducer, such as mode frequencies and amplitude ratios of the mode shapes, are determined following Galerkin method. The response of the transducer under the four electric sources with 90° phase difference is then obtained by the modal summation method. With the results, the performance of the transducer under the electric sources can be estimated. The present work provides a general and precise theoretical modelling on the dynamical movement of the transducer.     

Observation of geometric phases for mixed states using NMR interferometry

Examples of geometric phases abound in many areas of physics. They offer both fundamental insights into many physical phenomena and lead to interesting practical implementations. One of them, as indicated recently, might be an inherently fault-tolerant quantum computation. This, however, requires one to deal with geometric phases in the presence of noise and interactions between different physical subsystems. Despite the wealth of literature on the subject of geometric phases very little is known about this very important case. Here we report the first experimental study of geometric phases for mixed quantum states. We show how different they are from the well-understood, noiseless, pure-state case.     

合肥光源逐圈束流位置监测系统中的定时系统

 定时系统是合肥光源逐圈束流位置监测和相空间测量系统中的重要组成部分,其主要目的是为数据采集卡提供与环内电子束团同步的时钟信号。该系统包含高速ECL时钟成形、分频电路、程控延时电路、控制模块等部分。可实现延时范围0～220ns,最小延时步距0.5ns,调整精度0.1ns,时钟抖动小于200ps。系统控制软件基于客户/服务器结构,操作灵活、方便。     

光学读出微梁阵列红外成像及性能分析

在构建的光学读出微梁阵列(焦平面阵列FPA)非制冷红外成像系统中，实现了无硅基底FPA置于空气中对人体的热成像. 通过FPA在不同真空度环境条件下的成像结果进行比较，分析了热导和系统噪声值随气压变化的关系，以及对系统成像性能的影响，并对气体分子热运动自由程大于空气传热层特征尺度时的气体热传导模型进行了修正分析和实验验证. 实验结果表明：FPA置于空气中时，气体分子撞击微梁引起的微梁反光板无序振动产生的光学读出噪声成为系统噪声的主要来源. 当真空度小于1Pa时，总热导和光学读出噪声值的变化都趋于平缓；当真空度小于10^-2Pa时，空气热导的影响可忽略，总热导降低到微梁感热像素的辐射极限，光学读出噪声也降低到一极小值. 实验结果与理论分析相符合. 关键词： 非制冷红外成像 光学读出 双材料微梁阵列 热导